A solution blow spinning (SBS) process was utilized to create nanofibers of TiO2/C and TiO2/C/N with potential applications in photocatalysis and dye adsorption. Polyvinylpyrrolidone was used as a carbon and nitrogen source. Their content in the TiO2 structure decreased as the temperature increased from 350 to 550 °C. Physical-chemical, morphological, and structural features were investigated. Adsorption and photodegradation experiments revealed that the material calcined at 400 °C had higher dye removal (98%) under dark settings, whereas the greater photodegradation efficiency under visible and UV light was 56% and 98%, respectively, for the sample calcined at 550 °C. The results suggest that the SBS has the potential to develop an efficient adsorbent and photocatalyst for use in treatments of contaminated water. (SBS TiO2C TiOC C TiO TiO2CN TiOCN N adsorption source 35 55 Physicalchemical, Physicalchemical Physical chemical, chemical Physical-chemical morphological investigated 40 98% 98 (98% settings 56 respectively water CN 3 5 4 9 (98 (9 (

A highly efficient NiFe2O4/TiO2 nanofibrous photocatalyst was prepared by a simultaneous solution blow spinning method. The hybrid fibers were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), Raman spectroscopy, and magnetometry. The photocatalytic properties were evaluated using Crystal violet (CV) and Congo red (CR) dyes under visible light irradiation. Fibers calcined at 600 ºC and 700 ºC showed the highest CV decolorization (77%). On the other hand, for CR, the best performance was encountered with the photocatalysts heat-treated at 500 ºC, which exhibited photocatalytic degradation of 87% after only 30 min of visible light irradiation. The high reaction rates (0.018 to 0.067 min-1) explain the fast decolorization yielded by the combined effect of adsorption and photocatalytic processes. Moreover, recyclability assays showed stable CR dye efficiency after five recycling cycles. Therefore, the NiFe2O4/TiO2 nanofibers present a high potential for application in the decolorization treatment of wastewater from the textile industry. NiFe2O4TiO2 NiFeOTiO NiFe2O4 TiO2 NiFe O TiO NiFe2O4/TiO method SEM, SEM , (SEM) Xray X ray XRD, XRD (XRD) spectroscopy magnetometry (CV (CR irradiation 60 70 77%. 77 77% . (77%) hand heattreated heat treated 50 87 3 0.018 0018 0 018 (0.01 0067 067 0.06 min1 1 min-1 processes Moreover cycles Therefore industry NiFe2O4TiO NiFeO NiFe2O (SEM (XRD 6 7 (77% 5 8 0.01 001 01 (0.0 006 06 0.0 min- (77 00 (0. 0. (7 (0 (