RESUMO A cirurgia paraendodontica é um procedimento que visa resolver problemas que nao poderiam ser resolvidos, ou quando nao é possível realizar o tratamento endodontico convencional. O objetivo deste estudo experimental foi comparar a microinfiltragao apical de dentes seccionados a 45° ou 90° em relagao ao longo eixo do dente e extremidade radicularpreenchida com agregado de trióxido mineral (MTA) utilizando estereomicroscopia. Neste estudo, 26 incisivos centrais superiores foram utilizados. Limpeza e modelagem foram realizadas com o uso da técnica de Oregon e as amostras foram divididas aleatoriamente em dois grupos. No Grupo A (n = 10) foi realizada segao apical em ángulo de 90°, realizando retrocavidade com ponta ultrassonica e retrobturagao com MTA. No grupo B (n = 10), os mesmos procedimentos foram realizados, mas a segao apical estava em um ángulo de 45°. Em seguida, as amostras foram imersas em um corante (nanquim), colocadas em estufa a 37°Cpor 48 h, antes da aplicagao da técnica de clareamento. Posteriormente, os dentes foram avaliados por estereomicroscópio, com aumento de 20x, para análise do vazamento de corante. Os dados foram submetidos ao teste t de Student, com nivel de significáncia p <0,05. Houve diferenga estatisticamente significante entre os grupos. O grupo B apresentou maiores valores de microinfil-tragao apical em comparagao ao grupo A (P = 0,004), mas ambos os grupos apresentaram vazamento de corante. Os resultados mostraram que a segao apical de 90° promoveu menores valores de microinfiltragao de corante na interface do material retrobturador dentinário do que a segao 45° e pode ser considerada a técnica mais efetiva para preparo apical em cirurgia paraendodontica.

ABSTRACT Paraendodontic surgery is a procedure that aims to solve problems that could not be solved by, or when it is not possible to perform conventional endodontic treatment. The aim of this experimental study was to compare the apical microleakage of teeth sectioned at 45° or 90° to the long axis of the tooth and root-end filled with mineral trioxide aggregate (MTA) using stereomicroscopy. In this study, 26 maxillary central incisors were used. Cleaning and shaping were performed with use of the Oregon technique and the samples were randomly divided into two groups. In Group A (n=10) apical section was performed at an angle of 90°, making a retrocavity with an ultrasonic tip and retrofilling with MTA. In group B (n=10) the same procedures were performed, but the apical section was at a 45° angle. Then the samples were immersed in a dye (India ink), placed in an oven at 37° for 48 h before applying the clearing technique. Afterwards the teeth were assessed by stereomicroscope at 20x magnification to analyze dye leakage. Data were submitted to the Student's-t test with significance level p<0.05. There was statistically significant difference between groups. Group B showed higher apical microleakage values compared with group A (P=0.004), but both groups showed dye leakage. The results showed that the 90° apical section promoted lower dye microleakage values at the dentin-retrofilling material interface than the 45°-section and could be considered the most effective technique for apical preparation in paraendodontic surgery.

Abstract Glucose production from sugarcane bagasse was investigated. Sugarcane bagasse was pretreated by four different methods: combined acid and alkaline, combined hydrothermal and alkaline, alkaline, and peroxide pretreatment. The raw material and the solid fraction of the pretreated bagasse were characterized according to the composition, SEM, X-ray and FTIR analysis. Glucose production after enzymatic hydrolysis of the pretreated bagasse was also evaluated. All these results were used to develop relationships between these parameters to understand better and improve this process. The results showed that the alkaline pretreatment, using sodium hydroxide, was able to reduce the amount of lignin in the sugarcane bagasse, leading to a better performance in glucose production after the pretreatment process and enzymatic hydrolysis. A good xylose production was also observed.

O principal método reconhecido pelos metrologistas para a avaliação da incerteza de medição é de facto o Guia para a Expressão da Incerteza de Medição (Guia ISO). Entretanto, devido a algumas limitações do método proposto pelo Guia ISO, a ISO desenvolveu um método suplementar para a avaliação da incerteza de medição baseado na propagação de funções de densidade de probabilidade através do método de Monte Carlo (ISO-S1). O presente artigo visa discutir esses métodos de quantificação da incerteza de medição. Os autores realizam uma revisão da literatura focando nos principais artigos que apresentam essas abordagens modernas, bem como discutem os méritos e as limitações de ambos os métodos. Além disso, um estudo comparativo entre os métodos foi realizado através de dois estudos de caso. Os resultados obtidos mostraram que é necessário avaliar a influência do grau de não linearidade na estimativa da incerteza antes de optar por quaisquer um dos métodos

The main method recognized by the metrologists for the evaluation of measurement uncertainty is de facto the Guide to the Expression of Uncertainty in Measurement (ISO Guide). Due to some limitations of the proposed method by ISO Guide however, ISO has developed a supplementary method for evaluating the measurement uncertainty based on the propagation of probability density functions using the Monte Carlo method (ISO-S1). The present paper discusses these methods for the quantification of measurement uncertainty. We review the literature, in particular the main papers presenting these modern approaches. We also discuss the merits and the limitations of the ISO Guide and ISO-S1 approaches. Furthermore, a comparative study between these two methods was carried out in two case studies. The obtained results show that it is necessary to evaluate the influence of the degree of non linearity in order to estimate the measurement uncertainty before either method is chosen

The study of dental implant surfaces is relevant in order to better understand the interaction of the titanium surface and the surrounding tissues. Clinical success is achieved not only because of implant material but also because of other properties as implant design, surface treatment and quality. In this work, we report a detailed surface investigation of three major Brazilian made implants and compared them to a world-known implant. The surface composition and morphology were investigated by using X-ray photoelectron spectroscopy and scanning electron microscopy. Results of a biological test implemented in order to verify the bioactivity of the implant surface are also presented.