Resumo Introdução Pinos de fibra de vidro são utilizados para melhorar a retenção das restaurações em dentes tratados endodonticamente. Objetivo Avaliar a resistência de união de pinos de fibra de vidro submetidos a diferentes tratamentos superficiais e cimentados à dentina radicular com cimento resinoso autoadesivo. Material e método trinta raízes de caninos humanos foram preparadas e divididas de acordo com dois fatores: tratamentos de superfície (silano, peróxido de hidrogênio a 35% ou bicarbonato de sódio) e o terço radicular (cervical e médio). Os pinos de fibra de vidro foram cimentados com cimento resinoso autoadesivo (RelyX U200) e foram divididos de acordo com duas regiões: cervical e terço médio. Após 24 horas, foram preparados para microtração (formato de ampulheta), padrão de fratura e avaliação micromorfológica por microscopia eletrônica de varredura, para medir a linha de cimento. Resultado Os dados (MPa e µm) foram submetidos à ANOVA two-way e teste de Tukey (α = 5%). Os tratamentos de superfície influenciaram a resistência de união dos pinos. A média da resistência de união (desvio padrão) diferiu de acordo com a região da dentina radicular (p <0,00): a região cervical (Controle: 19,16Mpa (3.71); Silano: 25,65MPa (4.04); Peróxido de hidrogênio: 24,43MPa (3.16); Bicarbonato de sódio: 37,42MPa (8.27)) apresentou valores de resistência a raiz (Controle: 14,66MPa (4.65); Silano: 12,52MPa (5.03); peróxido de hidrogênio: 10,64MPa (3.33); bicarbonato de sódio: 10,87MPa (2.49)). Conclusão O tratamento com agentes químicos e físicos aumentou a resistência de união da interface cimento-pino-dentina no terço cervical e o tratamento com bicarbonato de sódio apresentou melhores resultados na resistência de união.

Abstract Introduction Glass-fiber posts are used in order to improve the retention of restorations in endodontically treated teeth. Objective To evaluate the bond strength of glass-fiber posts submitted to different surface treatments and cemented to the root canal dentin with self-adhesive resin cement. Material and method Thirty roots of human canines were prepared and divided according to two factors: surface treatments (silane, 35% hydrogen peroxide, or sodium bicarbonate) and root thirds (cervical and middle thirds). The glass-fiber posts were cemented with self-adhesive resin cement (RelyX U200). After 24 h, the specimens were prepared for microtensile bond strength test (hourglass format), fracture pattern and micromorphological assessment by scanning electronic microscopy, in order to measure the cement line. Result The data (MPa and µm) were submitted to two-way ANOVA and Tukey’s test (α = 5%). The surface treatments influenced the bond strength of the posts cemented with self-adhesive resin cement (p<0.00). The mean bond strength (standard deviations) differed according to the region of root dentin (p<0.00): the cervical region (Control: 19.16MPa (3.71); Silane: 25.65MPa (4.04); Hydrogen peroxide: 24.43MPa (3.16); Sodium bicarbonate: 37.42MPa (8.27)) showed higher bond strength values than the middle third of the root (Control: 14.66MPa (4.65); Silane: 12.52MPa (5.03); Hydrogen peroxide: 10.64MPa (3.33); Sodium bicarbonate: 10.87MPa (2.49)). Conclusion Treatment of the glass-fiber post surface with chemical and physical agents increased the bond strength of the cement-post-dentin interface in the cervical third and the treatment with Sodium bicarbonate showed better results in bond strength.

Resumo Este estudo retrospectivo comparou a taxa de falha anual (TFA), razões para falha e fatores influenciadores da sobrevida de restaurações posteriores e anteriores de resina composta realizadas por estudantes de graduação. As restaurações deveriam estar em oclusão, com pelo menos um dente adjacente, e os pacientes deveriam ter comparecido a pelo menos 1 consulta anual de retorno. A investigação foi realizada em 2 analises separadas: 1) dados odontológicos de prontuário eletrônico de pacientes (n=333 restaurações) foram selecionados para avaliar os fatores influenciadores na sobrevida; 2) avaliação de 30 pacientes por exame clinico das restaurações (n=123) para verificar as características clinicas e a distribuição do tipo de falha. Os dados foram submetidos a Kaplan-Meier método, Log-rank teste, regressão de Cox e Teste Exato de Fisher (p<0,05). Após o período de 8 anos, a TFA foi 2,62%. Houve diferença entre restaurações anteriores e posteriores (p=0,005), sendo que anteriores mostraram maior TFA. Os fatores de risco à carie (p<0,001) e o número de superfícies restauradas (p=0,010) influenciaram a sobrevida de restaurações. Brilho superficial (p=0,029), fratura (p=0,025) e retenção (p=0,011) foram critérios clínicos com diferenças entre restaurações anteriores e posteriores. Renda (p<0,001), atividade de cárie (p<0,001), risco à cárie (p<0,001) e risco oclusal (p<0,001) também influenciaram a sobrevida. Após 8 anos, a TFA das restaurações realizadas por estudantes de graduação foram clinicamente aceitáveis e afetadas pelos fatores de risco associados ao pacientes e a posição do dente na arcada; restaurações anteriores falham mais do que posteriores.

Abstract This retrospective study aimed to compare the annual failure rate (AFR), reasons for failure and factors influencing survival of posterior and anterior composite restorations placed by undergraduate students. Composite restorations placed by undergraduate students were evaluated. The restorations should be in occlusion, with at least one adjacent tooth; and patients should have been present for check-up, with at least 1 annual recall. The investigation was performed in two separate analysis: 1) dental electronic records of 100 patients (n=333 restorations) were selected to assess factors influencing survival; 2) clinical evaluation of 30 patients by examining restorations (n=123) to assess clinical characteristics and failure type distribution. Data were subjected to Kaplan-Meier method, Log-rank test, Cox regression and Fisher’s Exact test (p<0.05). After 8-year period, the AFR was 2.62%. There was difference between anterior and posterior restorations (p=0.005), with anterior showing a higher AFR. The patient caries-risk (p<0.001) and the number of surfaces restored (p=0.010) affected restoration survival. The superficial brightness (p=0.029), fracture (p=0.025) and retention (p=0.011) were clinical criteria with differences between anterior and posterior restorations. Income (p<0.001), caries activity (p<0.001), caries risk (p<0.001) and oclusal risk (p<0.001) also influenced on the restorations survival. After 8-year, the AFR of restorations placed by undergraduate students was acceptable and affected by patient risk factors and the position of the tooth in the arch: anterior restorations failed more than posterior.

Abstract Objectives: To evaluate the effects of dentin pretreatment and temperature on the bond strength of a universal adhesive system to dentin. Material and Methods: Ninety-six extracted non-carious human third molars were randomly divided into 12 groups (n=8) according to Scotchbond Universal Adhesive (SbU) applied in self-etch (SE) and etch-and-rinse (ER) mode, adhesive temperature (20°C or 37°C) and sodium bicarbonate or aluminum oxide air abrasion. After composite build up, bonded sticks with cross-sectional area of 1 mm2 were obtained to evaluate the microtensile bond strength (μTBS). The specimens were tested at a crosshead speed of 0.5 mm/min on a testing machine until failure. Fractured specimens were analyzed under stereomicroscope to determine the failure patterns in adhesive, cohesive (dentin or resin) and mixed fractures. The microtensile bond strength data was analyzed using two-way ANOVA and Tukey's test (α=5%). Results: Interaction between treatment and temperature was statistically significant for SbU applied in self-etch technique. Both dentin treatments showed higher bond strength for ER mode, regardless of adhesive temperature. When compared to control group, sodium bicarbonate increased bond strength of SbU in SE technique. Adhesive temperature did not significantly affect the μTBS of tested groups. Predominantly, adhesive failure was observed for all groups. Conclusions: Dentin surface treatment with sodium bicarbonate air abrasion improves bond strength of SbU, irrespective of adhesive application mode, which makes this approach an alternative to increase adhesive performance of Scotchbond Universal Adhesive to dentin.

Resumo Objetivo Avaliar a influência da dentina afetada na resistência de união de um sistema adesivo universal e de um adesivo de condicionamento ácido total acetonado. Material e método As faces oclusais de 60 terceiros molares humanos, hígidos e cariados, foram removidas a fim de expor o substrato dentinário. Os dentes foram divididos aleatoriamente em 6 grupos: Single Bond Universal (3M Dental Products, Seefeld, Germany), nos protocolos de condicionamento total e autocondicionante, e Prime&BondNT (DentsplyDeTrey, Konstanz, Germany), em dentina hígida e afetada. A smearlayer de 30 espécimes de dentina hígida foi padronizada com lixas de granulação 600. A dentina residual infectada de 30 espécimes foi removida com uma broca carbide número 4 até que nada fosse detectável por uma inspeção clínica. Pinos de resina composta (Filtek Z350 XT, 3M ESPE, St. Paul, MN) foram construídos usando tubos de amido como matriz. O teste de microcisalhamento foi realizado em uma máquina universal de testes até que houvesse a fratura. Resultado Diferenças significantes foram observadas na resistência de união apenas para os espécimes de dentina afetada. A resistência de união do Single Bond Universal não foi influenciada pelo protocolo de aplicação nos espécimes de dentina hígida, mas diminuiu para os espécimes de dentina afetada, enquanto que o desempenho da adesão do Prime&BondNT não foi influenciada pela condição dentinária. Conclusão A dentina afetada reduziu a resistência de união do Single Bond Universal, em comparação à dentina hígida. A resistência de união do Prime & Bond NT não foi alterada pela condição dos substratos.

Abstract Objective To evaluate the influence of caries-affected dentin on bond strength of a universal one-step and a multi-step etch-and-rinse adhesive system. Material and method Enamel of 60 third human molars with and without caries was removed to expose dentin. The teeth were randomly assigned to six groups: Single Bond Universal (3M ESPE, St. Paul, MN, USA) in etch-and-rinse and in self-etch mode and Prime & Bond NT (Dentsply Co, Konstanz, Germany), all on sound and caries-affected dentin. Smear layer of the 30 sound dentin specimens was standardized by polishing with 600-grit SiC paper under water cooling. Residual infected dentin of the 30 caries-affected specimens was removed with a number 4 CA carbide bur until no caries smooth tissue was detectable by tactile-visual inspection. Cylinders of a light cured composite resin (Filtek Z350 XT, 3M ESPE) were built up using starch tubes and microshear test was performed until failure. The data was analyzed by one-way ANOVA and Tukey’s post hoc test. Result Significant differences in microshear bond strength (μSBS) were observed for the caries-affected groups, but not for sound dentin. The μSBS of Single Bond Universal were not influenced by the application protocol on sound dentin, however they were lower in the caries-affected group with both application protocols. The μSBS for Prime & Bond NT was not influenced by the dentin conditions. Conclusion Caries-affected dentin decrease in bond strength of Single Bond Universal in comparison to sound dentin. The bond strength of Prime & Bond NT was not altered by substrate conditions.

Resumo Introdução O aumento da temperatura do adesivo tem sido pesquisado como forma de melhorar a evaporação do solvente, reduzir a viscosidade e melhorar a permeação dos monômeros na dentina. Objetivo Investigar a influência de diferentes métodos de aquecimento na resistência de união à dentina sob um ensaio de microtração de um adesivo de condicionamento ácido total. Material e método Vinte e quatro terceiros molares hígidos foram seccionados transversalmente a fim de expor a superfície plana da dentina. As amostras foram condicionadas ácido fosfórico a 37% e dividido em três grupos (n=8). São eles: 1) Controle - onde o adesivo (Adper Single Bond 2, 3M ESPE) foi aplicado em temperatura normal (25°C); 2) Dispositivo de aquecimento – O adesivo foi aquecido em um dispositivo específico até alcançar a temperatura de 37°C e só então aplicado à dentina; 3) Ar quente – Usou-se jato de ar aquecido a 50°C por 10 segundos a uma distância de 10cm para facilitar a evaporação do solvente. Os espécimes foram restaurados com resina composta (Filtek Z250 A2, 3M ESPE) e preparados para o ensaio de microtração, após 24h de armazenamento em água destilada. Os dados obtidos foram submetidos para análise de variância (ANOVA) e teste de Tukey (p<0,05). Resultado Não houve diferença significativa entre os grupos (p>0,05). As médias da resistência de união para o grupo controle, dispositivo de aquecimento e ar quente foram, respectivamente, 48,5 (± 5,2), 40,35 (± 4,9), e 47,2 (± 5,3). Conclusão Os diferentes métodos de aquecimento não influenciaram significativamente na resistência de união imediata à dentina de um Sistema adesivo de condicionamento ácido total.

Abstract Introduction Increased adhesive temperature has been reported to promote solvent evaporation, reduce viscosity, and improve monomeric permeation into dentin. Objective The aim of this study was to determine the influence of different heating methods on the microtensile bond strength of an etch-and-rinse adhesive to dentin. Material and method Twenty-four caries-free extracted human third molars were transversally sectioned to expose a flat dentinal surface. The samples were etched with 37% phosphoric acid gel and divided into three groups (n = 8): 1) Control - the adhesive system (Adper Single Bond 2; 3M ESPE) was applied at room temperature; 2) Warming device - the adhesive was warmed to 37°C in a custom device before application; and 3) Warm air - the adhesive was warmed to 50°C with an air jet after application on dentin. The specimens were restored with a composite resin (Filtek Z250 A2, 3M ESPE) and prepared for microtensile bond strength testing, after 24 h in water storage. The data were subjected to one-way ANOVA and Tukey's test (p < 0.05). Result There was no significant difference among the groups (p > 0.05). The mean bond strength values in the control, the warming device, and the warm air groups were 48.5 (± 5.2), 40.35 (± 4.9), and 47.2 (± 5.3) MPa, respectively (p = 0.05). Conclusion The different heating methods had no significant influence on the immediate microtensile bond strength of an etch-and-rinse ethanol-based adhesive to dentin.

The adhesive systems are responsible for an efficient union between teeth and resin, resulting in a longevity restoration. They are organic molecules di or multifunctional that contain reactive groups that interact with dentin and with the resin monomer of composite resin. The adhesive systems are characterized by wet adhesion, which is a result of presence of hidrophylics radicals in their compositions, to promote a better bond and the best properties of the adhesion. Adhesive systems may use two different strategies to interact with the dental structure: total-etching and self-etching technique. The total-etching systems require a conditioning, a rinsing and a priming step in order to allow involvement of collagen fibers by the resin monomers and the formation of the so-called ‘hybrid layer’. The total-etching promotes the cleaning of dentin, also promotes superficial demineralization and delivers collagen fibrils to participate of an interface union mechanism teeth/ adhesive system/restorative material. Self-etching adhesive systems are characterized by demineralization and infiltration of resin monomers simultaneously. This technique is attractive because reduced sensitivity associated with retaining the smear layer and smear plugs, thereby, minimize the possibility of inadvertent contamination of the bonding surface with dentinal surface through dentinal fluid transudate.

Los sistemas adhesivos son responsables de una unión eficaz entre los dientes y la resina, dando como resultado una restauración durable. Son moléculas orgánicas bi o multifuncionales que contienen grupos reactivos que interactúan con la dentina y con el monómero de resina de composite. Los sistemas adhesivos se caracterizan por la adhesión húmeda, que es el resultado de la presencia de radicales hidrofílicos en sus composiciones, para promover una mejor adherencia y las mejores propiedades de la adhesión. Los sistemas adhesivos pueden utilizar dos estrategias diferentes para interactuar con la estructura dental: Técnica de grabado total y auto-grabado. Los sistemas de grabado total requiere un acondicionamiento, un lavado y un paso de priming con el fin de permitir la participación de las fibras de colágeno por los monómeros de resina y la formación de la llamada capa híbrida. El grabado total promueve la limpieza de la dentina, también promueve la desmineralización superficial y condiciona a las fibrillas de colágeno para participar de un mecanismo de interfaz de unión diente/sistema adhesivo /material de restauración. Los sistemas adhesivos autograbantes se caracterizan por la desmineralización y la infiltración de los monómeros de resina de forma simultánea. Esta técnica es atractiva debido a la sensibilidad reducida asociada a conservar la capa de barro dentinario y tapones de barro dentinario, reduciendo al mínimo la posibilidad de contaminación accidental de la superficie de unión con la superficie de la dentina a través del líquido dentinario trasudado.

Cuando el factor estética es primordial, las resinas compuestas continúan siendo la opción restauradora más utilizada. Sin embargo, a pesar de su constante evolución aún presentan algunos inconvenientes, tales como: desgaste, contracción de polimerización e infiltración marginal. Actualmente, nuevos conceptos relacionados a técnicas de fotopolimerización desarrollaron una mejor adaptación marginal asociada a la permanencia de sus propiedades mecánicas. La polimerización gradual, es decir, reducción inicial de la intensidad de luz, seguida por fotoactivación con mayor intensidad han demostrado ser una alternativa con buenos resultados clínicos. Este trabajo propone discutir las principales variables que pueden interferir en el proceso de fotopolimerización, con el objetivo de alertar a los odontólogos en cuanto a la necesidad de un constante control clínico, no solamente por la observación de la técnica incremental, sino principalmente, a través de la monitorización de la cantidad de energía luminosa empleada en el proceso de fotopolimerización. En este contexto, son presentados, mediante revisión de literatura, los principales factores relacionados a la contracción de polimerización y las técnicas de fotopolimerización disponibles para minimizar sus efectos.

The composite resins are still the most used restorative option when the esthetic aspect is primordial. However, even their constant evolution they present some inconvenients like: wear, polymerization contraction and marginal leakage. Today, new concepts related to light curing have developed a better marginal adaptation associated to the permanency of their mechanical properties. The gradual polymerization, which means, initial reduction at the light intensity, followed by the photoactivation with more intensity has demonstrated to be an alternative with good clinical results. This paper proposes to discuss the principal variables that could interfere at the light curing process, with the aim to alert the dentists about the necessity of a constant clinical control, not just by the observation of the incremental technique, but principally, through monitoring the quantity of light energy used at the polymerization process. In this context, are presented, by a literature revision, the principal factors related to the polymerization contraction and the available light curing techniques to minimize their effects.

This study evaluated comparatively by scanning electron microscopy (SEM) the effect of different dental conditioners on dentin micromorphology, when used according to the same protocol. Forty dentin sticks were obtained from 20 caries-free third human molars and were assigned to 4 groups corresponding to 3 conditioners (phosphoric acid 37%, Clearfil SE Bond and iBond) and an untreated control group. After application of the conditioners, the specimens were immersed in 50% ethanol solution during 10 s, chemically fixed and dehydrated to prepare them to SEM analysis. In the control group, dentin surface was completely covered by smear layer and all dentinal tubules were occluded. In the phosphoric acid-etched group, dentin surface was completely clean and presented exposed dentinal tubule openings; this was the only group in which the tubules exhibited the funnel-shaped aspect. In the groups conditioned with Clearfil SE Bond primer and iBond, which are less acidic than phosphoric acid, tubule openings were occluded or partially occluded, though smear layer removal was observed. SE Bond was more efficient in removing the smear layer than iBond. In the Clearfil SE Bond group, the cuff-like aspect of peritubular dentin was more evident. It may be concluded all tested conditioners were able to change dentin morphology. However, it cannot be stated that the agent aggressiveness was the only cause of the micromorphological alterations because a single morphological pattern was not established for each group, but rather an association of different aspects, according to the aggressiveness of the tested conditioner.

O uso de condicionadores ácidos para desmineralizar a superfície dental e expor a rede de fibras colágenas para interdifusão dos monômeros adesivos e conseqüente formação da camada híbrida tem sido considerado o mais eficiente mecanismo de adesão dos agentes de união. O objetivo deste estudo foi comparar a resistência de união à dentina de três sistemas adesivos, dois autocondicionantes (Clearfil SE Bond - CSEB e One Up Bond F - OUBF) e um de condicionamento total (Single Bond - SB), sob três diferentes condições de substrato dentinário (úmido, seco e reidratado). Noventa terceiros molares humanos recém-extraídos foram cortados na superfície oclusal, para se remover o esmalte e formar uma parede plana de dentina. Os espécimes foram restaurados com resina composta (Filtek Z250) e submetidos ao teste de resistência de união à tração (TBS) em uma MTS 810. As médias foram submetidas à ANOVA a dois critérios e ao teste de Tukey (p = 0,05). A dentina úmida apresentou os maiores valores de TBS para os sistemas adesivos SB e CSEB. A dentina seca e a reidratada apresentaram TBS significativamente menor quando foi empregado SB. OUBF não apresentou resultados influenciados pela condição do substrato dentinário, tendo produzido TBS similares para os diferentes tratamentos de superfície.

The use of acid etchants to produce surface demineralization and collagen network exposure, allowing adhesive monomers interdiffusion and consequently the formation of a hybrid layer, has been considered the most efficient mechanism of dentin bonding. The aim of this study was to compare the tensile bond strength to dentin of three adhesive systems, two self-etching ones (Clearfil SE Bond - CSEB and One Up Bond F - OUBF) and one total-etching one (Single Bond - SB), under three dentinal substrate conditions (wet, dry and re-wet). Ninety human, freshly extracted third molars were sectioned at the occlusal surface to remove enamel and to form a flat dentin wall. The specimens were restored with composite resin (Filtek Z250) and submitted to tensile bond strength testing (TBS) in an MTS 810. The data were submitted to two-way ANOVA and Tukey's test (p = 0.05). Wet dentin presented the highest TBS values for SB and CSEB. Dry dentin and re-wet produced significantly lower TBS values when using SB. OUBF was not affected by the different conditions of the dentin substrate, producing similar TBS values regardless of the surface pretreatments.