Abstract Glass ceramics’ fractures in zirconia fixed dental prosthesis (FDP) remains a clinical challenge since it has higher fracture rates than the gold standard, metal ceramic FDP. Nanoindentation has been shown a reliable tool to determine residual stress of ceramic systems, which can ultimately correlate to failure-proneness. Objectives: To assess residual tensile stress using nanoindentation in veneered three-unit zirconia FDPs at different surfaces of pontics and abutments. Methodology: Three composite resin replicas of the maxillary first premolar and crown-prepared abutment first molar were made to obtain three-unit FDPs. The FDPs were veneered with glass ceramic containing fluorapatite crystals and resin cemented on the replicas, embedded in epoxy resin, sectioned, and polished. Each specimen was subjected to nanoindentation in the following regions of interest: 1) Mesial premolar abutment (MPMa); 2) Distal premolar abutment (DPMa); 3) Buccal premolar abutment (BPMa); 4) Lingual premolar abutment (LPMa); 5) Mesial premolar pontic (MPMp); 6) Distal premolar pontic (DPMp); 7) Buccal premolar pontic (BPMp); 8) Lingual premolar pontic (LPMp); 9) Mesial molar abutment (MMa); 10) Distal molar abutment (DMa); 11) Buccal molar abutment (BMa); and 12) Lingual molar abutment (LMa). Data were assessed using Linear Mixed Model and Least Significant Difference (95%) tests. Results: Pontics had significantly higher hardness values than premolar (p=0.001) and molar (p=0.007) abutments, suggesting lower residual stress levels. Marginal ridges yielded higher hardness values for connectors (DPMa, MMa, MPMp and DPMp) than for outer proximal surfaces of abutments (MPMa and DMa). The mesial marginal ridge of the premolar abutment (MPMa) had the lowest hardness values, suggesting higher residual stress concentration. Conclusions: Residual stress in three-unit FDPs was lower in pontics than in abutments. The outer proximal surfaces of the abutments had the highest residual stress concentration.

OBJECTIVES: The aim of this study was to investigate the internal fit (IF) of glass-infiltrated alumina (ICA - In-Ceram Alumina), yttria-stabilized tetragonal zirconia polycrystals (Y-TZP - IPS e.max ZirCAD), and metal-ceramic (MC - Ni-Cr alloy) crowns. MATERIAL AND METHODS: Sixty standardized resin-tooth replicas of a maxillary first molar were produced for crown placement and divided into 3 groups (n=20 each) according to the core material used (metal, ICA or Y-TZP). The IF of the crowns was measured using the replica technique, which employs a light body polyvinyl siloxane impression material to simulate the cement layer thickness. The data were analyzed according to the surfaces obtained for the occlusal space (OS), axial space (AS) and total mean (TM) using two-way ANOVA with Tukey ’s multiple comparison test (p<0.05). RESULTS: No differences among the different areas were detected in the MC group. For the Y-TZP and ICA groups, AS was statistically lower than both OS and TM. No differences in AS were observed among the groups. However, OS and TM showed significantly higher values for ICA and Y-TZP groups than MC group. Comparisons of ICA and Y-TZP revealed that OS was significantly lower for Y-TZP group, whereas no differences were observed for TM. CONCLUSIONS: The total mean achieved by all groups was within the range of clinical acceptability. However, the metal-ceramic group demonstrated significantly lower values than the all-ceramic groups, especially in OS.

The wear resistance of denture teeth is important to the longevity of removable prostheses of edentulous patients. The ability of denture teeth to maintain a stable occlusal relationship over time may be influenced by this property. The purpose of this in vitro study was to evaluate the wear resistance of polymethyl methacrylate (PMMA) denture teeth based on their chemical composition when opposed by a ceramic antagonist. The maxillary canines (n=10) of 3 PMMA denture teeth (Trubyte Biotone, cross-linked PMMA; Trilux, highly cross-linked IPN (interpenetrating polymer network)-PMMA; and Vivodent, highly cross-linked PMMA) were secured in an in vitro 2-body wear-testing apparatus that produced sliding contact of the specimens (4.5 cycles/s, sliding distance of 20 mm, under 37°C running water) against glazed or airborne particle abraded ceramic. Wear resistance was measured as height loss (mm) under 300 g (sliding force) after 100,000 cycles, using a digital measuring microscope. Mean values were analyzed by 2-way ANOVA and Tukey's test (a=0.05). The wear of Trubyte Biotone (0.93 ± 0.14 mm) was significantly higher than that of both other types of teeth tested against abraded ceramic (p<0.05). The Vivodent tooth (0.64 ± 0.17 mm) exhibited the best wear resistance among the denture teeth tested against airborne particle abraded ceramic. There were no statistically significant differences (p>0.05) in wear among the 3 denture teeth evaluated against glazed ceramic. Trilux and Vivodent teeth tested against either glazed or airborne particle abraded ceramic did not differ significantly from each other (p<0.05). All teeth showed significantly more wear against airborne particle abraded ceramic than against glazed ceramic (p<0.05). In conclusion, the three types of PMMA denture teeth presented significantly different wear resistance against the abraded ceramic. The high-strength PMMA denture teeth were more wear-resistant than the conventional PMMA denture tooth.

A seleção adequada do agente cimentante é essencial para evitar falhas por perda de retenção em coroas retidas por núcleos. O objetivo deste estudo foi investigar a resistência à tração e o tipo de falha de pinos de fibra de vidro cimentados com diferentes materiais. Cimentaram-se pinos de fibra de vidro em 40 pré-molares inferiores, divididos em 4 grupos (n = 10): Grupo 1 - ionômero de vidro modificado por resina RelyX Luting; Grupo 2 - ionômero de vidro modificado por resina Fuji Plus; Grupo 3 - cimento resinoso RelyX ARC; Grupo 4 - cimento resinoso Enforce. Avaliaram-se os espécimes por teste de resistência à tração e análise por microscopia óptica para observação do tipo de falha. Compararam-se os valores de resistência à tração de cada grupo por análise de variância e teste de Tukey, sendo que o nível de significância estabelecido foi de 5%. Descreveram-se os tipos de falha na forma de porcentagens. Os valores de resistência à tração obtidos foram: Grupo 1 - 247,6 N; Grupo 2 - 256,7 N; Grupo 3 - 502,1 N; Grupo 4 - 477,3 N. Não houve diferença estatisticamente significativa entre os Grupos 1 e 2 ou entre os Grupos 3 e 4, porém os cimentos resinosos apresentaram valores de resistência à tração significativamente maiores do que os apresentados pelos cimentos ionoméricos. O Grupo 1 exibiu 70% de falhas coesivas, enquanto os Grupos 2, 3 e 4 apresentaram 70% a 80% de falhas adesivas na interface dentina-cimento. Concluiu-se que os cimentos resinosos e ionoméricos são capazes de proporcionar retenção clinicamente suficiente de pinos de fibras de vidro, e que os cimentos ionoméricos podem ser indicados principalmente quando houver dificuldades de aplicar técnicas adesivas.

Proper selection of the luting agent is fundamental to avoid failure due to lack of retention in post-retained crowns. The objective of this study was to investigate the tensile bond strength and failure mode of glass fiber posts luted with different cements. Glass fiber posts were luted in 40 mandibular premolars, divided into 4 groups (n = 10): Group 1 - resin-modified glass ionomer RelyX Luting; Group 2 - resin-modified glass ionomer Fuji Plus; Group 3 - resin cement RelyX ARC; Group 4 - resin cement Enforce. Specimens were assessed by tensile strength testing and light microscopy analysis for observation of failure mode. The tensile bond strength values of each group were compared by ANOVA and Tukey test. The significance level was set at 5%. The failure modes were described as percentages. The following tensile strength values were obtained: Group 1 - 247.6 N; Group 2 - 256.7 N; Group 3 - 502.1 N; Group 4 - 477.3 N. There was no statistically significant difference between Groups 1 and 2 or between Groups 3 and 4, yet the resin cements presented significantly higher tensile bond strength values than those presented by the glass ionomer cements. Group 1 displayed 70% of cohesive failures, whereas Groups 2, 3 and 4 exhibited 70% to 80% of adhesive failures at the dentin-cement interface. We concluded that resin cements and glass ionomer cements are able to provide clinically sufficient retention of glass fiber posts, and that glass ionomer cements may be especially indicated when the application of adhesive techniques is difficult.

Muitos profissionais utilizam restaurações metalocerâmicas sem atentarem para as características de compatibilidade entre metal e cerâmica, fator muito importante para o sucesso deste tipo de restauração. Este estudo avaliou a resistência de união entre uma liga de paládio-prata (Pors-on 4) e 3 cerâmicas (Ceramco, Noritake e Vita VMK-68) aplicando-se forças de cisalhamento na interface metal/porcelana. Uma matriz especialmente desenvolvida serviu para a confecção dos corpos-de-prova e realização dos testes de cisalhamento. Trinta corpos-de-prova foram confeccionados, com duas camadas de cerâmica opaca e de corpo, e os testes realizados em máquina universal de ensaios (0,5 mm/min). As médias de resistência de união (em MPa) foram: 28,21 (Ceramco), 28,96 (Noritake) e 24,11 (Vita VMK-68). A análise de variância a um critério não demonstrou diferença estatisticamente significante entre os materiais (p>0,05). Os resultados demonstraram que todas as cerâmicas foram compatíveis com a liga avaliada.

Dentists and technicians have used dental ceramics associated with different types of alloys without taking into account the characteristics of compatibility of these materials. Knowing the properties of the alloy and ceramic used in metal/ceramic restorations is a key factor for treatment success. The purpose of this study was to evaluate the bond strength of a palladium-silver alloy (Pors-on 4) to 3 ceramics (Ceramco, Noritake and Vita VMK-68) using shear forces at the metal-ceramic interface. A stainless steel cylindrical matrix was used for preparation of the metal dies, application of ceramic and shear strength testing. Thirty palladium-silver alloy cylinders received two layers of opaque and two layers of body porcelain, and shear tests were performed in a universal testing machine at a cross-head speed of 0.5 mm/min. Shear bond strength means (in MPa) were: 28.21(Ceramco), 28.96 (Noritake) and 24.11 (Vita VMK-68). One-way ANOVA did not show statistically significant differences (p>0.05) among the materials. The results of this study indicate that the three evaluated ceramic systems are suitable to be used in combination with the tested palladium-silver alloy.

OBJETIVO: O objetivo do estudo foi investigar a resistência à fratura sob compressão e padrão de falha de pré-molares tratados endodonticamente e clareados internamente por 21 dias com peróxido de carbamida a 37%, aplicando-se diferentes procedimentos restauradores. MATERIAL E MÉTODOS: O objetivo deste estudo foi investigar a resistência à fratura sob compressão e padrão de falha de pré-molares unirradiculares tratados endodonticamente e clareados internamente com peróxido de carbamida a 37%. Foram constituídos 6 grupos (n = 10): 1) dentes sem clareamento e câmara pulpar vedada com IRM; 2) dentes clareados e câmara pulpar vedada com IRM; 3) dentes clareados e câmara pulpar preenchida com resina composta fotopolimerizável; 4) dentes clareados, condutos preparados com 10mm, e preenchimento do conduto e câmara pulpar com IRM; 5) dentes clareados, condutos preparados com 10mm, cimentação de pino metálico pré-fabricado com fosfato de zinco e câmara pulpar vedada com resina composta; 6) dentes clareados, condutos preparados com 10mm, cimentação de pino de fibra de vidro com cimento resinoso e câmara pulpar vedada com resina composta. Após 24 horas de armazenamento em água destilada, os espécimes foram submetidos ao teste de resistência à fratura sob compressão em máquina de ensaios universal. RESULTADOS: Os seguintes valores foram encontrados: grupo 1 - 56,23kgf; grupo 2 - 48,96kgf; grupo 3 - 53,99kgf; grupo 4 - 45,72kgf; grupo 5 - 54,22kgf; grupo 6 - 60,12kgf. A Análise de Variância não mostrou diferença estatisticamente significante entre os grupos (p < .05), sugerindo que o clareamento interno com peróxido de carbamida a 37% não enfraqueceu os tecidos dentais. O maior número de fraturas desfavoráveis foi encontrado nos grupos 2 (50%), 4 (40%), e 5 (30%). O grupo 6 exibiu o padrão de falhas mais favorável. CONCLUSÃO: Os resultados sugerem que o clareamento interno com peróxido de carbamida a 37% não causou enfraquecimento importante dos dentes. Entre os dentes clareados, aqueles com restaurações temporárias de IRM ou com pinos metálicos mostraram o padrão mais desfavorável de fratura, enquanto o padrão de fratura mais favorável ocorreu em dentes restaurados com resina composta e pinos de fibras de vidro.

OBJECTIVE: This study investigated the compressive fracture strength and failure pattern in premolars submitted to endodontic treatment and internal bleaching with 37% carbamide peroxide for 21 days, with application of different restorative procedures. MATERIAL AND METHODS: Six groups were employed (n = 10): 1) non-bleached teeth and pulp chamber sealed with IRM; 2) bleached teeth and pulp chamber sealed with IRM; 3) bleached teeth and pulp chamber filled with light cured composite resin; 4) bleached teeth, root canals prepared at 10mm, filling of the root canal and pulp chamber with IRM; 5) bleached teeth, root canals prepared at 10mm, luting of prefabricated metallic post with zinc phosphate and pulp chamber sealed with composite resin; 6) bleached teeth, root canals prepared at 10mm, luting of glass fiber post with resin cement and pulp chamber sealed with composite resin. After 24-hour storage in distilled water, the specimens were submitted to compressive fracture strength testing in a universal testing machine. RESULTS: The following values were found: Group 1 - 56.23kgf; Group 2 - 48.96kgf; Group 3 - 53.99kgf; Group 4 - 45.72kgf; Group 5 - 54.22kgf; Group 6 - 60.12kgf. The analysis of variance did not reveal statistically significant difference between groups (p<0.05), suggesting that internal bleaching with 37% carbamide peroxide did not weaken the dental tissues. The largest number of unfavorable fractures was observed for Groups 2 (50%), 4 (40%), and 5 (30%). Group 6 exhibited the most favorable failure pattern. CONCLUSIONS: The results suggest that internal bleaching with 37% carbamide peroxide did not significantly weaken the teeth. Among the bleached teeth, those with temporary IRM restorations or metallic posts demonstrated the most unfavorable fracture pattern, whereas the most favorable fracture pattern occurred in teeth restored with composite resin and glass fiber posts.

O objetivo desta pesquisa foi avaliar a influência do remanescente dentário coronal de dentes tratados endodonticamente, restaurados com pinos pré-fabricados e duas resinas como núcleos de preenchimento, uma de presa dual (Enforce Core) e outra fotopolimerizável (Z-250). Foram utilizados 40 caninos superiores humanos extraídos, divididos em quatro grupos de 10 espécimes: Grupo l - com remanescente dentário coronal de 3mm e restaurados com Enforce Core; Grupo ll - com remanescente dentário coronal de 3mm e restaurado com Z-250; Grupo III - sem remanescente dentário coronal e restaurado com Enforce Core; Grupo IV - sem remanescente dentário coronal e restaurado com Z-250. Após restaurados, os dentes foram levados a uma Máquina de Ensaio Universal e submetidos a uma força de compressão à 45º até que ocorresse fratura da restauração. A análise dos resultados (ANOVA, p>0,05) mostrou não haver diferença estatisticamente significativa entre os dentes com e sem remanescente dentário coronal. Com relação ao material utilizado para o preenchimento coronário, constatou-se diferença significativa, sendo que os valores mais elevados de resistência à fratura foram encontrados no grupo restaurado com a resina fotopolimerizável.

OBJECTIVES: The aim of this study was to evaluate the influence of remaining coronal tooth structure on endodontically treated teeth restored with prefabricated posts and two different composites for core build-up: dual-cured resin (Enforce Core) and light-cured resin (Z-250). METHODS: Fourty freshly extracted canines were endodontically treated and divided into four groups: Group I - teeth with 3mm remaining coronal structure, restored with Enforce Core; Group II - teeth with 3mm remaining coronal structure, restored with Z-250; Group III - teeth with no remaining coronal structure, restored with Enforce; Group IV - teeth with no remaining coronal structure, restored with Z-250. After restoration, the teeth were embedded in acrylic resin and the fracture resistance was measured on a universal testing machine at 45 degrees to the long axis of the tooth until failure. RESULTS: Data were analyzed by two-way analysis of variance, which showed significant differences between groups (p=0.00). The Tukey test did not show significant differences between specimens with and without remaining coronal structure. Conversely, significant difference was observed between groups with different core build-up. The highest values of fracture resistance were found in the group restored with light-cured resin. SIGNIFICANCE: The remaining coronal tooth structure did not influence the resistance of endodontically treated teeth; however, the change of core build-up was able to modify this resistence.

O objetivo deste trabalho foi avaliar a influência do número e localização de padrões de resina para fundição de núcleos metálicos fundidos (NMF), na reprodução do diâmetro e comprimento dos pinos. Foram confeccionados 72 padrões de resina utilizando pinos plásticos pré-fabricados e divididos para fundição em 3 grupos: G1- anel pequeno/4padrões, G2- anel médio/6 padrões e G3-anel grande/8 padrões. Metade deles foi posicionada à direita da linha média do anel e metade à esquerda, servindo de orientação para posicionar o anel na centrífuga. Através do microscópio comparador foram obtidas medidas antes e depois da fundição, tanto do comprimento quanto do diâmetro em diferentes locais. Os resultados foram submetidos à análise estatística (ANOVA a dois critérios e Tukey), possibilitando as seguintes observações: 1°) a posição dos padrões não exerceu influência nas dimensões mensuradas. 2°) o mesmo ocorreu com a quantidade de padrões dentro do anel. 3°) apenas em relação ao diâmetro (3 e 6mm) dos pinos do grupo G3, houve diferença estatisticamente significante. Conclui-se que: 1°) a posição do padrão dentro do anel e o número de padrões não resultou em alteração significativa do comprimento e diâmetro dos pinos. 2°) A variação de diâmetro (3, 6, e 9mm) foi significante apenas para os pinos do grupo G3.

The aim of this study was the evaluation about the influence of the quantity and the localization of resin patterns to cast metallic posts in its diameter and length reproduction. Seventy-two patterns for posts were fabricated by using prefabricated FKG plastic posts and divided for casting in 3 groups: G1-small ring/4 patterns, G2- medium ring/6 patterns, G3- big ring/8 patterns. Half of the patterns of each group were placed on the right side of the ring midline and the other half, on the left side, in order to guide the ring inside of the centrifuge. Using the comparative microscope, measures of diameter and length in different places were obtained before and after casting. The results were submitted to statistic analysis (ANOVA two way and Tukey's test), to make possible these observations: 1°) the position of patterns didn't influenced the measured dimensions. 2°) the same happened with the quantity of patterns inside the ring. 3°) only the pins of group G3 have presented statistically significant diameter differences. In conclusion, 1°) the position of patterns inside the ring and its quantity did not result in significant changes in pins length and diameter. 2°) Although there were no significant length alterations, significant ones were observed in the diameters 3, 6, and 9mm of Group G3.

O protocolo para prótese sobre implantes recomenda o uso de uma infra-estrutura em ouro para próteses metalo-plásticas e metalo-cerâmicas. No entanto, devido ao seu alto custo, o uso de ligas alternativas é desejado. OBJETIVO: Este estudo compara a adaptação marginal de cilindros protéticos pré-fabricados e cilindros protéticos plásticos fundidos com dois tipos de ligas metálicas básicas. MATERIAL E MÉTODOS: 05 amostras de (1) cilindros plásticos fundidos em liga de cobalto cromo; (2) cilindros plásticos fundidos em liga de níquel cromo e (3) cilindros pré-fabricados com cinta metálica em paládio, foram examinados na interface intermediário/cilindro protético na análise de desajuste marginal, considerando-se (A) desajuste vertical, (B) desajuste horizontal e (C) profundidade de fenda. RESULTADOS: os valores médios para o desajuste vertical, horizontal e profundidade foram, respectivamente, 4,13µm, 14,5µm e 6,93µm para o cilindro pré-fabricado em paládio, 23,18µm, 33,2µm e 88µm para os cilindros plásticos fundidos em Níquel cromo e 25,6µm, 51,8µm e 114,54 µm para os cilindros fundidos em cobalto-cromo. CONCLUSÃO: não foram encontradas diferenças estatísticas entre os grupos fundidos (grupo 1 e 2), mas uma adaptação marginal significantemente superior foi observada com os cilindros pré-fabricados quando comparado aos cilindros plásticos fundidos com níquel-cromo e cobalto-cromo para todas as análises.

The original protocol for implant prosthesis recommends the use of a gold framework for acrylic and ceramic prosthesis. However, due to its high cost, the use of alternative alloys is desired. This study compares the marginal accuracy of pre-made cylinders versus plastic cylinders cast with two different base metal casting alloys. Five samples each of (1) plastic cylinder cast in cobalt-chromium alloy, (2) plastic cylinder cast in nickel-chromium alloy, and (3) silver-palladium pre-made cylinder (control) were examined for marginal accuracy according to: (A) vertical gap; (B) horizontal gap and (C) horizontal gap depth at the abutment/cylinder interface. Data were submitted to statistical analysis (ANOVA and Student-Newman Keuls, p<0.05). Mean values for vertical, horizontal and gap depth were 4.13µm, 14.5µm and 6.93µm for pre-made cylinder, 23.18µm, 33.2µm and 88µm for Ni-Cr cast cylinder and 25.6µm, 51.8µm and 114.54µm for Co-Cr cast cylinder. No statistically significant differences were found between cast groups (1 and 2), but significant better fit was obtained with pre-made metal cylinders when compared to cast cylinders with Ni-Cr and Co-Cr alloys, for all analyses.

Este estudo avaliou a resistência ao cisalhamento da união porcelana/resina, usando 40 corpos-de-prova cilíndricos de metal + porcelana + resina composta quer foram divididos em 4 grupos, de acordo com o tratamento superficial da porcelana: 1) sem tratamento, 2) retenções mecânicas feitas com ponta diamantada, 3) ataque ácido com ácido fosfórico + silano, 4) ataque ácido com ácido fluorídrico + silano. Após uma semana de armazenamento em água destilada à temperatura ambiente, os espécimes foram submetidos à carga de cisalhamento e os dados analisados estatisticamente (ANOVA). As médias dos grupos foram em MPa: 4.71 (grupo 1); 4.81 (grupo 2); 11.76 (grupo 3) e 11.07 (grupo 4). Não houve diferenças estatisticamente significantes entre os grupos 1 e 2 e entre os grupos 3 e 4.

This study evaluated the shear bond strength of porcelain/composite using 40 metal + porcelain + composite cylindrical specimens divided into 4 groups, according to porcelain surface treatment: 1) no treatment, 2) mechanical retentions performed with diamond burs, 3) etching with phosphoric acid+silane, and 4) etching with hydrofluoric acid+silane. After being stored in distilled water at room temperature for one week, the specimens were submitted to a shear force (load) and the data were analyzed statistically (ANOVA). The means (in Mpa) of the groups were: 4.71 (group 1); 4.81 (group 2); 11.76 (group 3); 11.07 (group 4). There were no statistically significant differences between groups 1 and 2 and between groups 3 and 4.

Avaliou-se a resistência de união metal/porcelana utilizando-se uma liga de Ni-Cr, submetida a diferentes tempos de oxidação prévia com o sistema cerâmico Vita-VMK, através do teste preconizado por CHIODI NETTO3. A análise dos resultados permitiu as seguintes conclusões: a ausência da oxidação prévia possibilitou os melhores resultados, sendo que a diferença foi estatisticamente significante; diferentes tempos de oxidação prévia provocaram redução acentuada nos valores obtidos e foram semelhantes entre si; o grupo submetido ao processo de jateamento após a oxidação prévia por cinco minutos mostrou resultados similares aos grupos que também passaram pelo processo de oxidação e não sofreram jateamento posterior.

The objective of this research was to evaluate the porcelain-alloy bonding strength using a local-made alloy under different times of pre-oxidation with a ceramic system. The test used was preconized by CHIODI NETTO. The results lead to the following conclusions: the control group (no pre-oxidation) showed the best values, statistically significant, when compared with others groups. The different times of pre-oxidation procedures reduced the values significantly, and the groups were similar to each other. The group submitted to the sandblasting process after a pre-oxidation of 5 minutes, showed similar values when compared with the other groups treated with pre-oxidation without sandblasting.